N-Methylaniline → HCID 23454949, 화합물

반응식

CNC1C=CC=CC=1.C(NNC1C=CC(N=C=S)=CC=1)=O.[CH:22]([NH:24][NH:25][C:26]1[CH:31]=[CH:30][C:29]([NH:32][C:33]([N:35]([CH2:43][C:44]2[CH:49]=[CH:48][CH:47]=[CH:46]C=2)[CH2:36]C2C=CC=CC=2)=[S:34])=[CH:28][CH:27]=1)=[O:23]>>[CH:22]([NH:24][NH:25][C:26]1[CH:27]=[CH:28][C:29]([NH:32][C:33]([N:35]([CH3:36])[C:43]2[CH:44]=[CH:49][CH:48]=[CH:47][CH:46]=2)=[S:34])=[CH:30][CH:31]=1)=[O:23]

참가 물질

반응물 3

HCID 7515N-Methylaniline

HCID 20283022N'-(4-Isothiocyanatophenyl)formohydrazide

HCID 23454956HCID 23454956, 화합물

생성물 1

HCID 23454949HCID 23454949, 화합물

실험 절차

N-Methylaniline (0.11 g, 0.001 mole) and 4-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.15 g (50 percent), m.p. 137°-139° C.

출처 및 근거

ORD 기록: ord-c0ded4a75eef4888b62f3bf7d16569f8
출처 데이터셋: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04276364

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