Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chlorocyclohexanone → 2,3-Dimethyl-2,3,5,6,7,8-hexahydro-1,4-benzodithiine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chlorocyclohexanone | HCID 13203 | — |
| 반응물 | 2,3-Butanedithiol | HCID 548353 | — |
| 생성물 | 2,3-Dimethyl-2,3,5,6,7,8-hexahydro-1,4-benzodithiine | HCID 12920054 | 49% |
반응 단계
The procedure of Example 1(a) is followed using 2,3-butanedithiol and 2-chlorocyclohexanone to give 5,6,7,8-tetrahydro-2,3-dimethyl-1,4-benzodithian as a greenish oil, b.p. 90°-100°/0.07 mm. Yield 49%. NMR 1.34 (6d), 1.45-2.25 (8m), 2.7-3.1 (2m). IR 2900, 1610, 1435, 1365, 1320, 1115, 795, 690.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04276422 |
| 출처 데이터셋 | uspto-grants-1981_06 |
| ORD ID | ord-9e166fd43ffd49b1bf660592ba6af3fe |
| 출처 메모 | uspto-grants-1981_06 |