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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1681348생성일: 2026년 10월 27일

(R,R)-Stilbene oxide → alpha-Phenyl-beta-[[2-(phenylmethoxy)propyl]amino]benzeneethanol

https://huagongshe.com/reaction/1681348

반응식

참여 물질

역할이름HCID투입량
반응물(R,R)-Stilbene oxideHCID 185583—
반응물2-(Benzyloxy)propan-1-amineHCID 296015—
생성물alpha-Phenyl-beta-[[2-(phenylmethoxy)propyl]amino]benzeneethanolHCID 1980638975.2%

반응 조건

온도140 °C

반응 단계

A mixture of trans-stilbene oxide (1.96 g, 0.010 mol) and 2-benzyloxypropylamine (2.48 g, 0.015 mol) was heated at 140° C. for 6 hours and then allowed to stand at ambient temperature for 12 hours. The solidified reaction mixture was triturated with petroleum ether and filtered to obtain 2.72 g of a solid. Mass spectral analysis showed starting materials present. Recrystallization from isooctane gave 2.16 g (60%) of the product as a white solid; mp 114°-119° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05171753
출처 데이터셋uspto-grants-1992_12
ORD IDord-439ae5a08b1241f3abeadb21b0bafc7d
출처 메모uspto-grants-1992_12