참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Styrene Oxide | HCID 7276 | — |
| 반응물 | 2-(Benzyloxy)propan-1-amine | HCID 296015 | — |
| 생성물 | alpha-[[[2-(Phenylmethoxy)propyl]amino]methyl]benzenemethanol | HCID 19806395 | 84.1% |
반응 단계
A mixture of styrene oxide (1.96 g, 0.010 mol) and 2-benzyloxypropylamine (2.48 g, 0.15 mol) was heated at 140° C. for 6 hours and then allowed to cool to ambient temperature and stand for 12 hours. The solidified reaction mixture was triturated with isooctane and filtered to obtain an impure solid that was recrystallized from isooctane to obtain 2.40 g of a white solid (84% yield); mp 90°-100° C. (undefined).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05171753 |
|---|
| 출처 데이터셋 | uspto-grants-1992_12 |
|---|
| ORD ID | ord-9930972b977f40ce97126d92214321de |
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| 출처 메모 | uspto-grants-1992_12 |
|---|
