Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Acetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ethylbenzene | HCID 7500 | — |
| 반응물 | Sodium Sulfite | HCID 24437 | — |
| 반응물 | Lead nitrate | HCID 24924 | — |
| 생성물 | Acetophenone | HCID 7410 | 95% |
반응 단계
Ten millimoles of ethylbenzene were heated at 400° C. for 1 hour with 1.35 ml of water containing 20 millimoles of sodium sulfite and 10 millimoles of lead nitrate. On cooling, a suspension of black precipitate was observed. The reaction product was extracted with ether and the ether layer was dried over Na2SO4 and concentrated to yield acetophenone in more than 95% yield. Acetophenone was confirmed by NMR and gas chromatographic techniques.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05171880 |
| 출처 데이터셋 | uspto-grants-1992_12 |
| ORD ID | ord-f2ef92410e4545f4b0b37e77be1d5962 |
| 출처 메모 | uspto-grants-1992_12 |