Dimethylamine → HCID 19382159, 화합물

반응식

[O:1]1[C:3]2([CH2:8][CH2:7][N:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[CH2:5][CH2:4]2)[CH2:2]1.[CH3:14][NH:15][CH3:16]>>[CH3:14][N:15]([CH2:2][C:3]1([OH:1])[CH2:8][CH2:7][N:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[CH2:5][CH2:4]1)[CH3:16]

참가 물질

반응물 2

HCID 674Dimethylamine

HCID 13672926Ethyl 1-oxa-6-azaspiro[2,5]octane-6-carboxylate

생성물 1

HCID 19382159HCID 19382159, 화합물

실험 절차

5.2 g (28 mmol) of ethyl 6-aza-1-oxaspiro[2,5]octane-6-carboxylate are added dropwise to 30 ml of dimethylamine solution (40% in water ) and the mixture is stirred overnight at room temperature. It is then concentrated and distilled.

후처리

concentrationIt is then concentrated
distillationdistilled

출처 및 근거

ORD 기록: ord-4ec812f6a6b14988bdc5f76b6568a65c
출처 데이터셋: uspto-grants-1992_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05173484

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