Nitric Acid → 2,4-Dichloro-3-nitrobenzoic acid

HRID 1682150노트

반응식

HRID 1682150 반응식
[N+:1]([O-:4])(O)=[O:2].[Cl:5][C:6]1[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9]>S(=O)(=O)(O)O>[Cl:5][C:6]1[C:14]([N+:1]([O-:4])=[O:2])=[C:13]([Cl:15])[CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9]

참가 물질

4

반응물 2

HCID 944Nitric AcidHCID 57872,4-Dichlorobenzoic Acid

생성물 1

HCID 190232292,4-Dichloro-3-nitrobenzoic acid

시약·촉매·용매 1

HCID 1118Sulfuric Acid용매

실험 절차

To a solution of 25 ml of fuming nitric acid and 20 ml of sulfuric acid, 25 g of 2,4-dichlorobenzoic acid was gradually added. After completion of the heat generation, the reaction mixture was poured into ice water. Precipitated solid was washed with water and dried to obtain 23.0 g of the desired product.

후처리

  1. customPrecipitated solid
  2. washwas washed with water
  3. customdried

출처 및 근거

ORD 기록
ord-e8fb074dc0314d3da49e00c91f786941
출처 데이터셋
uspto-grants-1992_12
특허 번호
US05175299

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