Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dimethylaniline → Methyl N-(2,6-dimethylphenyl)-DL-alaninate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dimethylaniline | HCID 6896 | — |
| 반응물 | Metalaxyl | HCID 42586 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | Alpha-bromopropionate | HCID 14535398 | — |
| 생성물 | Methyl N-(2,6-dimethylphenyl)-DL-alaninate | HCID 94555 | — |
반응 단계
The preparation of metalaxyl is published in the CH-PS 607,888, according to which 2,6-dimethylaniline is first reacted with methyl DL-α-bromopropionate in the presence of sodium hydrogen carbonate as acid binding agent, then methyl N-(2,6-dimethylphenyl)-DL-alaninate thus obtained is acylated with methoxyacetyl chloride to give metalaxyl.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05639905 |
| 출처 데이터셋 | uspto-grants-1997_06 |
| ORD ID | ord-477b7476c77943e99d6ea4ee8b9d3031 |
| 출처 메모 | uspto-grants-1997_06 |