Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Heptanedione, 6-methyl- → 4-(3,4-Dimethoxyphenyl)-3-isovaleryl-6,7-dimethoxy-2-methylquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Heptanedione, 6-methyl- | HCID 76354 | — |
| 반응물 | 2-Amino-3',4',4,5-tetramethoxybenzophenone hydrochloride | HCID 21466134 | — |
| 생성물 | 4-(3,4-Dimethoxyphenyl)-3-isovaleryl-6,7-dimethoxy-2-methylquinoline | HCID 19039903 | — |
반응 단계
According to the same manner as that described in Reference Example 6, 2-amino-3',4',4,5-tetramethoxybenzophenone hydrochloride was reacted with 6-methyl-2,4-heptanedione to give 4-(3,4-dimethoxyphenyl)-3-isovaleryl-6,7-dimethoxy-2-methylquinoline. This compound was recrystallized from ethyl acetate-hexane to give colorless prisms. mp. 135°-137° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05641788 |
| 출처 데이터셋 | uspto-grants-1997_06 |
| ORD ID | ord-ab1656257a47449eb2535eb25de22302 |
| 출처 메모 | uspto-grants-1997_06 |