3,5-Dimethyl-4-hydroxybenzaldehyde → HCID 178426652, 화합물

HRID 1685704노트

반응식

HRID 1685704 반응식
[CH2:1]([C:3]1[CH:8]=[C:7]([C:9](=[NH:12])[NH:10][OH:11])[CH:6]=[C:5]([CH3:13])[C:4]=1[CH2:14][CH2:15][C:16]([OH:18])=[O:17])C.CC1C=C(C=C(C)C=1O)C=O>>[OH:11][NH:10][C:9]([C:7]1[CH:6]=[C:5]([CH3:13])[C:4]([CH2:14][CH2:15][C:16]([OH:18])=[O:17])=[C:3]([CH3:1])[CH:8]=1)=[NH:12]

참가 물질

3

반응물 2

HCID 752223,5-Dimethyl-4-hydroxybenzaldehydeHCID 178436623HCID 178436623, 화합물

생성물 1

HCID 178426652HCID 178426652, 화합물

실험 절차

The title compound is prepared in analogy to 3-[2-ethyl-4-(N-hydroxycarbamimidoyl)-6-methyl-phenyl]-propionic acid starting from 3,5-dimethyl-4-hydroxybenzaldehyde; LC-MS: tR=0.57 min, [M+1]+=237.02; 1H NMR (D6-DMSO): δ2.29 (s, 6H), 2.30-2.36 (m, 2H), 2.80-2.87 (m, 2H), 5.66 (s, 2H), 7.30 (s, 2H), 9.46 (s, 1H).

출처 및 근거

ORD 기록
ord-9e403cacf501447cae72d03a6ccb73bf
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08148410B2

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