4-Cyanobenzenesulfonyl chloride → HCID 178472928, 화합물

HRID 1685725노트

반응식

HRID 1685725 반응식
[OH:1][NH:2][C:3](=[NH:17])[C:4]1[CH:9]=[CH:8][C:7]([S:10](=[O:16])(=[O:15])NCCO)=[CH:6][CH:5]=1.C(C1C=CC(S(Cl)(=O)=O)=CC=1)#N.Cl.[CH2:31]([O:33][C:34](=[O:37])[CH2:35][NH2:36])[CH3:32]>>[CH2:31]([O:33][C:34](=[O:37])[CH2:35][NH:36][S:10]([C:7]1[CH:6]=[CH:5][C:4]([C:3](=[NH:17])[NH:2][OH:1])=[CH:9][CH:8]=1)(=[O:16])=[O:15])[CH3:32]

참가 물질

4

반응물 3

HCID 394974-Cyanobenzenesulfonyl chlorideHCID 2723640Glycine ethyl ester, hydrochlorideHCID 178513366HCID 178513366, 화합물

생성물 1

HCID 178472928HCID 178472928, 화합물

실험 절차

The title compound is prepared in analogy to N-hydroxy-4-(2-hydroxy-ethylsulfamoyl)-benzamidine starting from 4-cyano-benzenesulfonyl chloride and glycine ethyl ester hydrochloride; LC-MS: tR=0.27 min; [M+1]+=302.03;

출처 및 근거

ORD 기록
ord-fe9e811952e74c96a480ec9e3dd670f0
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08148410B2

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