Methanesulfonyl chloride → HCID 86643789, 화합물

HRID 1686134노트

반응식

HRID 1686134 반응식
[CH3:1][S:2](Cl)(=[O:4])=[O:3].[CH:6]1([CH2:12][CH2:13][CH:14]([OH:16])[CH3:15])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>C(Cl)Cl>[CH3:1][S:2]([O:16][CH:14]([CH3:15])[CH2:13][CH2:12][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)(=[O:4])=[O:3]

참가 물질

4

반응물 2

HCID 31297Methanesulfonyl chlorideHCID 112065alpha-Methylcyclohexanepropanol

생성물 1

HCID 86643789HCID 86643789, 화합물수율 107.5%

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

실험 절차

A solution of 3.53 g methanesulfonyl chloride in 100 mL methylene chloride was added to a solution of 4.38 g 4-cyclohexylbutan-2-ol in 200 mL methylene chloride. The reaction mixture was stirred over night. Aqueous work-up yielded 7.06 g (96%) of a colourless oil.

출처 및 근거

ORD 기록
ord-380e1845775c4597bf39768a151e6233
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08148538B2

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