1,3-dimethyl-1H-indole-2-carbaldehyde → HCID 22139134, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:4]=[CH:5][CH:6]=[C:7]2[C:11]=1[N:10]([CH3:12])[CH:9]=[C:8]2[CH:13]=O.[CH3:15][N:16]1C2C(=CC=CC=2)C(C)=C1C=O>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][CH:6]=[C:7]2[C:11]=1[N:10]([CH3:12])[CH:9]=[C:8]2[CH2:13][NH:16][CH3:15]

참가 물질

반응물 2

HCID 27714681,3-dimethyl-1H-indole-2-carbaldehyde

HCID 221390927-methoxy-1-methyl-1H-indole-3-carboxaldehyde

생성물 1

HCID 22139134HCID 22139134, 화합물수율 94%

실험 절차

According to the procedure of Preparation 13(c), except substituting 7-methoxy-1-methyl-1H-indole-3-carboxaldehyde for the 1,3-dimethyl-1H-indole-2-carboxaldehyde, the title compound (1.6 g, 94%) was obtained as an amber oil: MS (ES) m/e 205.2 (M+H)+.

출처 및 근거

ORD 기록: ord-aa481e1afd834b499c7623e38fdc9621
출처 데이터셋: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08153652B2

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