Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-chloro-1-methyl-1H-indole-3-carbaldehyde → 5-chloro-1-methyl-3-(methylaminomethyl)-1H-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-chloro-1-methyl-1H-indole-3-carbaldehyde | HCID 16723796 | — |
| 반응물 | Methyl 2-((5-bromopyridin-2-yl)amino)acetate | HCID 22139049 | — |
| 생성물 | 5-chloro-1-methyl-3-(methylaminomethyl)-1H-indole | HCID 22139017 | 93% |
반응 단계
According to the procedure of Preparation 13 (c), except substituting 5-chloro-1-methyl-1H-indole-3-carboxaldehyde for the, 3-dimethyl-1H-indole-2-carboxaldehyde, the title compound (2.1 g, 93%) was obtained as an amber oil: MS (ES) m/e 209.0 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08153652B2 |
| 출처 데이터셋 | uspto-grants-2012_04 |
| ORD ID | ord-03e83df8ed4a43e6a7572f082de34ea9 |
| 출처 메모 | uspto-grants-2012_04 |