4-Bromo-N,N-dimethylbenzenesulphonamide → HCID 11429045, 화합물

HRID 1694747

반응식

HRID 1694747 반응식
B([C:4]1[CH:15]=[C:14]([Cl:16])[CH:13]=[CH:12][C:5]=1[O:6][C@@H:7]([CH3:11])[C:8]([OH:10])=[O:9])(O)O.Br[C:18]1[CH:23]=[CH:22][C:21]([S:24]([N:27]([CH3:29])[CH3:28])(=[O:26])=[O:25])=[CH:20][CH:19]=1>C1COCC1>[Cl:16][C:14]1[CH:13]=[CH:12][C:5]([O:6][C@@H:7]([CH3:11])[C:8]([OH:10])=[O:9])=[C:4]([C:18]2[CH:19]=[CH:20][C:21]([S:24]([N:27]([CH3:29])[CH3:28])(=[O:25])=[O:26])=[CH:22][CH:23]=2)[CH:15]=1

참가 물질

4

반응물 2

HCID 128184-Bromo-N,N-dimethylbenzenesulphonamideHCID 67277298(2S)-2-(2-borono-4-chlorophenoxy)-propanoic acid

생성물 1

HCID 11429045HCID 11429045, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The title compound was prepared by the method of example 144 step (i) using the product from step (iv) and 4-bromo-N,N-dimethylbenzenesulfonamide and THF as solvent. Yield (0.068 g).

후처리

  1. customYield (0.068 g)

출처 및 근거

ORD 기록
ord-9b4d93441cba419b8d4b27d060596aed
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08158820B2

연결된 노트

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