(2S)-2-(2-borono-4-chlorophenoxy)-propanoic acid → HCID 58333648, 화합물

HRID 1694748

반응식

HRID 1694748 반응식
B([C:4]1[CH:15]=[C:14]([Cl:16])[CH:13]=[CH:12][C:5]=1[O:6][C@@H:7]([CH3:11])[C:8]([OH:10])=[O:9])(O)O.[Cl:17][C:18]1[CH:19]=[C:20]([S:25]([N:28]([CH3:30])[CH3:29])(=[O:27])=[O:26])[CH:21]=[CH:22][C:23]=1I>CO>[Cl:17][C:18]1[CH:19]=[C:20]([S:25]([N:28]([CH3:30])[CH3:29])(=[O:27])=[O:26])[CH:21]=[CH:22][C:23]=1[C:4]1[CH:15]=[C:14]([Cl:16])[CH:13]=[CH:12][C:5]=1[O:6][C@@H:7]([CH3:11])[C:8]([OH:10])=[O:9]

참가 물질

4

반응물 2

HCID 67277298(2S)-2-(2-borono-4-chlorophenoxy)-propanoic acidHCID 672802043-Chloro-4-iodo-N,N-dimethylbenzenesulfonamide

생성물 1

HCID 58333648HCID 58333648, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The title compound was prepared by the method of example 144 step (i) using the product from example 151 step (iv), the product from example 148 step (ii) and methanol as solvent. Yield (0.08 g).

후처리

  1. customYield (0.08 g)

출처 및 근거

ORD 기록
ord-58239a4d6a9a4aecbd462b5f965d84e1
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08158820B2

연결된 노트

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