HCID 178418443, 화합물 → HCID 178448981, 화합물

HRID 1694819노트

반응식

HRID 1694819 반응식
[CH2:1](/[N:5]=[CH:6]/[C:7]1[C:12]([F:13])=[CH:11][CH:10]=[CH:9][C:8]=1Cl)[CH2:2][CH2:3][CH3:4].[CH2:15]([Mg]Br)[CH3:16]>O1CCCC1.CCOCC>[CH2:1](/[N:5]=[CH:6]/[C:7]1[C:12]([F:13])=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:15][CH3:16])[CH2:2][CH2:3][CH3:4]

참가 물질

5

반응물 2

HCID 178418443HCID 178418443, 화합물HCID 178448982HCID 178448982, 화합물

생성물 1

HCID 178448981HCID 178448981, 화합물

시약·촉매·용매 2

HCID 3283Diethyl Ether용매HCID 8028Tetrahydrofuran용매

실험 절차

Prepared as described in Example 58(a) as by-product of reaction between butyl-[1-(2-chloro-6-fluoro-phenyl)-meth-(E)-ylidene]-amine and ethylmagnesium bromide in tetrahydrofuran and ether. MS (ISP): 208.3 ([M+H]+).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-643ac8ff08a34fe39b2f135de468359a
출처 데이터셋
uspto-grants-2012_04
특허 번호
US08158668B2

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