2-Propanol, 1-amino-2-methyl- → HCID 59846167, 화합물
반응식
[CH:1]([C:3]1[CH:8]=[CH:7][C:6]([S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1)=[O:2].C([O-])(O)=O.[Na+].[NH2:18][CH2:19][C:20]([CH3:23])([OH:22])[CH3:21]>CO>[CH:1]([C:3]1[CH:8]=[CH:7][C:6]([S:9]([NH:18][CH2:19][C:20]([OH:22])([CH3:23])[CH3:21])(=[O:11])=[O:10])=[CH:5][CH:4]=1)=[O:2]참가 물질
5
실험 절차
To a solution of 4-formyl-benzene sulfonyl chloride (1.0 g) in MeOH was added NaHCO3 (0.425 g), followed by 1-amino-2-methylpropan-2-ol (0.566 g). The reaction mixture was stirred for 1 h at RT, then filtered through Celite and the solvent removed under reduced pressure to provide 4-formyl-N-(2-hydroxy-2-methylpropyl)-benzene sulfonamide.
후처리
- filtrationfiltered through Celite
- customthe solvent removed under reduced pressure
출처 및 근거
- ORD 기록
- ord-84e19fda845941afaeadf147790c95b7
- 출처 데이터셋
- uspto-grants-2012_04
- 특허 번호
- US08163906B2
반응 노트
불러오는 중…