Dimethylformamide → 1-(2-Formyl-6-chloro-2,3,4,9-tetrahydro-1H-beta-carbolin-1-yl)cyclobutanecarboxamide
반응식
[ClH:1].Cl[C:3]1[CH:4]=[C:5]2[C:13](=[CH:14][CH:15]=1)[NH:12][C:11]1[CH:10]([C:16]3([C:20]([O:22]CC)=O)[CH2:19][CH2:18][CH2:17]3)[NH:9][CH2:8][CH2:7][C:6]2=1.[CH3:25][O-:26].[Na+].C[N:29](C)C=O>>[CH:25]([N:9]1[CH2:8][CH2:7][C:6]2[C:5]3[C:13](=[CH:14][CH:15]=[C:3]([Cl:1])[CH:4]=3)[NH:12][C:11]=2[CH:10]1[C:16]1([C:20]([NH2:29])=[O:22])[CH2:17][CH2:18][CH2:19]1)=[O:26]참가 물질
4
실험 절차
Reaction between the compound of Example 1 and aminocarbaldehyde in the presence of sodium methoxide in dimethylformamide enables the desired product to be obtained.
출처 및 근거
- ORD 기록
- ord-73254fc7f7fc48fda239f71de6616003
- 출처 데이터셋
- uspto-grants-2002_02
- 특허 번호
- US06350757B1
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