참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Chlorobenzotrichloride | HCID 21277 | — |
| 반응물 | Sulfur dichloride | HCID 25353 | — |
| 촉매 | Iron chloride (FeCl3) | HCID 24380 | — |
| 생성물 | 3,4-Dichlorophenyltrichloromethane | HCID 25608 | 51.4% |
반응 단계
A mixture of 57.5 g (250 mmol) of p-chlorobenzotrichloride, 1.5 g (9.2 mmol) of iron(III) chloride and 28 g (272 mmol) of sulphur dichloride was warmed to 80° C. for 3 hours. Thereafter, it was worked up in the manner indicated in Example 1. 34 g of 3,4-dichlorobenzotrichloride were thus obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04191711 |
|---|
| 출처 데이터셋 | uspto-grants-1980_03 |
|---|
| ORD ID | ord-8d0885b3be5147fdbd3f704b1cb056dd |
|---|
| 출처 메모 | uspto-grants-1980_03 |
|---|
