1-Pyrrolidineethanamine → 63207-76-1

HRID 1701336노트

반응식

HRID 1701336 반응식
[C:1]1([CH:7]([CH2:11][CH3:12])[C:8]([Cl:10])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:13]1([CH2:18][CH2:19][NH2:20])[CH2:17][CH2:16][CH2:15][CH2:14]1>C1C=CC=CC=1>[ClH:10].[N:13]1([CH2:18][CH2:19][NH:20][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:11][CH3:12])[CH2:17][CH2:16][CH2:15][CH2:14]1

참가 물질

4

반응물 2

HCID 13441-PyrrolidineethanamineHCID 981732-Phenylbutyryl chloride

생성물 1

HCID 304730863207-76-1

시약·촉매·용매 1

HCID 241Benzene용매2회

실험 절차

To a solution of 1 mol of α-phenyl-α-ethyl acetyl chloride in 2 liters of benzene add, with agitation, a benzene solution of 1 mol of 2-pyrrolidino-ethyl amine. The hydrochloric acid formed during condensation attaches itself to the pyrrolidine group and the expected derivative crystallizes out in the reaction medium.

출처 및 근거

ORD 기록
ord-12d744586784463982c45a0b0398ed9d
출처 데이터셋
uspto-grants-1980_03
특허 번호
US04192883

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