Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Eugenol → Methyleugenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Eugenol | HCID 3314 | — |
| 반응물 | Dimethyl Carbonate | HCID 12021 | — |
| 반응물 | Tributylphosphine | HCID 13831 | — |
| 생성물 | Methyleugenol | HCID 7127 | 88% |
반응 단계
33 parts of eugenol, 50 parts of dimethyl carbonate and 2 parts of tri-n-butylphosphine are kept for 15 hours at 190° C. Working up takes place as described in Example 24. 31 parts (88% of theory, based on converted eugenol) of eugenol methyl ether of boiling point 69°-70° C./0.13 mbar are obtained. The conversion is virtually quantitative.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04192949 |
| 출처 데이터셋 | uspto-grants-1980_03 |
| ORD ID | ord-e1b6aa7759434938a4f3748b71ae39bf |
| 출처 메모 | uspto-grants-1980_03 |