Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-Nitrothiazole → 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-Nitrothiazole | HCID 8486 | — |
| 반응물 | Benzoyl chloride, 3-nitro- | HCID 8495 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide | HCID 298930 | — |
반응 단계
By following the procedure of the first part of Example 1, but using m-nitrobenzoyl chloride (27.8 g), 2-amino-5-nitrothiazole (21.8 g) and pyridine (100 ml), there was obtained 3-nitro-N-(5-nitro-2-thiazolyl)benzamide, m.pt 200°-201°, after recrystallisation from acetic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04379156 |
| 출처 데이터셋 | uspto-grants-1983_04 |
| ORD ID | ord-869f3175addf4932a6aa8edebdad26e4 |
| 출처 메모 | uspto-grants-1983_04 |