Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-Nitrothiazole → 2-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-Nitrothiazole | HCID 8486 | — |
| 반응물 | 2-Nitrobenzoyl chloride | HCID 11875 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide | HCID 321578 | — |
반응 단계
By following the procedure of the first part of Example 1, but using 2-nitrobenzoyl chloride (18.5 g), 2-amino-5-nitrothiazole (14.5 g) and pyridine (ca 80 ml), there was obtained 2-nitro-N-(5-nitro-2-thiazolyl)-benzamide, m.pt 248°-250°, after crystallization from 2-methoxyethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04379156 |
| 출처 데이터셋 | uspto-grants-1983_04 |
| ORD ID | ord-cac03bb0ec004497bb492e2ec43f2cea |
| 출처 메모 | uspto-grants-1983_04 |