Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoacetamide → 2-((3-Nitrobenzoyl)imino)-5-nitro-3(2H)-thiazoleacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoacetamide | HCID 3727 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide | HCID 298930 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-((3-Nitrobenzoyl)imino)-5-nitro-3(2H)-thiazoleacetamide | HCID 3061827 | — |
반응 단계
By following the procedure of Example 5, but using a dispersion of sodium hydride (2.1 g 60% w/w) in mineral oil, 3-nitro-N-(5-nitro-2-thiazolyl)benzamide (11.8 g), N,N-dimethylformamide (100 ml) and 2-iodoacetamide (11.1 g), there was obtained 2-[(3-nitrobenzoyl)imino]-5-nitro-4-thiazoline-3-acetamide, m.pt 251°-252°, after recrystallization from pyridine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04379156 |
| 출처 데이터셋 | uspto-grants-1983_04 |
| ORD ID | ord-2349b54282b249599bf09d1921f4e09b |
| 출처 메모 | uspto-grants-1983_04 |