Ammonia → HCID 14770684, 화합물
반응식
[NH3:1].[C:2]([C:4]1[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:5]=1[S:11](Cl)(=[O:13])=[O:12])#[N:3]>O1CCOCC1.O>[NH2:3][C:2]1[C:4]2[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:5]=2[S:11](=[O:13])(=[O:12])[N:1]=1참가 물질
5
실험 절차
12.5 ml of 25% ammonia were added at approx. 60° C. to a solution of 11,8 g of 2-cyano-3-chlorobenzenesulphonylchloride in 20 ml of dioxane. After heating on a steam bath for 30 minutes the reaction mixture was cooled and diluted with water. The resulting crystalline product was sucked off, washed with water and dried. The desired product was obtained in a yield of 8.9 g. After recrystallization from ethanol, the product melted at 261°-263° C.
후처리
- temperatureAfter heating on a steam bath for 30 minutes the reaction mixture
- temperaturewas cooled
- washwashed with water
- customdried
출처 및 근거
- ORD 기록
- ord-e99cfa74832c44fb815b02e4a5c3827b
- 출처 데이터셋
- uspto-grants-1983_04
- 특허 번호
- US04379157
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