Ammonia → HCID 14770684, 화합물

반응식

Cl[C:2]1[C:6]2[C:7]([Cl:11])=[CH:8][CH:9]=[CH:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1.[NH3:14]>>[NH2:14][C:2]1[C:6]2[C:7]([Cl:11])=[CH:8][CH:9]=[CH:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1

참가 물질

반응물 2

HCID 222Ammonia

HCID 23320762HCID 23320762, 화합물

생성물 1

HCID 14770684HCID 14770684, 화합물

실험 절차

4.72 g of 3,4-dichlorobenzo[d]isothiazole-1,1-dioxide were added to 15 ml of 25% ammonia in 15 ml of ice water. After stirring at room temperature for two hours, the desired product was sucked off and dried; yield 4.20 g; melting-point 260° C.

출처 및 근거

ORD 기록: ord-03808e3111054a448940e21fa1ea82e4
출처 데이터셋: uspto-grants-1983_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04379157

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