Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → alpha-Bromo-3-chloropropiophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 3'-Chloropropiophenone | HCID 587128 | — |
| 생성물 | alpha-Bromo-3-chloropropiophenone | HCID 4992116 | — |
반응 단계
To 1 mole of m-chloropropiophenone heated to 85±5° C., bromine was added dropwise under stirring. The reaction temperature was kept at 85±5° C. during and after the addition of bromine, and the reaction was carried on for 2 hours. Then m-chloro-α-bromopropiophenone (compound of formula (II)) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737302B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-f3db7bb05d2f478a806fe6b5641ed89b |
| 출처 메모 | uspto-grants-2010_06 |