Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → N-(2-Chloro-3-pyridinyl)-1-methyl-4-nitro-1H-pyrazole-5-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-Chloro-3-pyridylamine | HCID 80528 | — |
| 반응물 | 1-Methyl-4-nitro-1H-pyrazole-5-carboxylic acid | HCID 592623 | — |
| 용매 | Hexamethylphosphoramide | HCID 12679 | — |
| 생성물 | N-(2-Chloro-3-pyridinyl)-1-methyl-4-nitro-1H-pyrazole-5-carboxamide | HCID 20503812 | — |
반응 단계
Prepared analogously to Example A(a) from 1-methyl-4-nitro-1H-pyrazole-5-carboxylic acid, thionyl chloride, and 2-chloro-3-aminopyridine in hexamethylphosphoric acid triamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04381303 |
| 출처 데이터셋 | uspto-grants-1983_04 |
| ORD ID | ord-b2a0c8d53a49410a83030612c2642573 |
| 출처 메모 | uspto-grants-1983_04 |