Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Chlorothiophenol → 4-(p-Chlorophenylthio)butyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Chlorothiophenol | HCID 7815 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1-Butanol, 4-chloro-, 1-acetate | HCID 23399 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-(p-Chlorophenylthio)butyl acetate | HCID 22762117 | — |
반응 단계
A mixture of 144.6 g of p-chlorothiophenol, 150.6 g of 4-chlorobutyl acetate, 80 g of 50% aqueous solution of sodium hydroxide and 750 ml of ethyl alcohol was heated under reflux for 5 hours. The alcohol was distilled off and ether was added to the cool mixture. After washing with dilute sodium hydroxide solution and then water, the ether solution was dried, evaporated to dryness and distilled. The product was collected at 110°-116° and 0.01 mm, ND25 1.5480.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04124723 |
| 출처 데이터셋 | uspto-grants-1978_11 |
| ORD ID | ord-d70fea656dfc4dd2a8e3c7cf3700a245 |
| 출처 메모 | uspto-grants-1978_11 |