3-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetate → HCID 22759281, 화합물

HRID 1704349노트

반응식

HRID 1704349 반응식
O1CCCCC1[O:7][CH2:8][C:9]#[C:10][CH:11]([O:21][C:22](=[O:24])[CH3:23])[CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1.O1CCCCC1OCCCC(OC(=O)C)COC1C=CC(F)=CC=1>>[C:22]([O:21][CH:11]([CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1)[C:10]#[C:9][CH2:8][OH:7])(=[O:24])[CH3:23]

참가 물질

3

반응물 2

HCID 227592583-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetateHCID 22759299HCID 22759299, 화합물

생성물 1

HCID 22759281HCID 22759281, 화합물

실험 절차

This compound is prepared by the procedure described in Example 4, Step B-5, except that 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)-2-pentyne (Example 4, Step B-3) is substituted for 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)pentane. The title compound is obtained as a light yellow oil which is not distilled but used directly in the next step.

후처리

  1. customThis compound is prepared by the procedure

출처 및 근거

ORD 기록
ord-40fa378b6863462f9a96c23260c3c3e5
출처 데이터셋
uspto-grants-1978_11
특허 번호
US04126629

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