Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyl Isothiocyanate → N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyl Isothiocyanate | HCID 7673 | — |
| 반응물 | 4-chloro-N-cyclopentylbenzylamine | HCID 834083 | — |
| 생성물 | N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea | HCID 13018271 | 92.8% |
반응 단계
Analogously to Example 1, 21 grams (0.1 mole) of N-4-chlorobenzyl-N-cyclopentylamine were reacted with 13.5 grams (0.1 mole) of phenylisothiocyanate. 32 grams of N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea were obtained. Yield: 92%, Melting point: 129°-132° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04127673 |
| 출처 데이터셋 | uspto-grants-1978_11 |
| ORD ID | ord-c45d45730c5d4b50b13b1fe0493dcdd3 |
| 출처 메모 | uspto-grants-1978_11 |