Methylamine → HCID 57178653, 화합물
반응식
O=[C:2]1[C:7]2[N:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][CH2:3]1.[CH3:11][NH2:12]>C(O)C>[CH3:11][N:12]=[C:2]1[C:7]2[N:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][CH2:3]1참가 물질
4
실험 절차
6 g (0.039 mole) of the ketone obtained in step (d) are dissolved in 50 ml anhydrous ethanol and treated for 30 minutes with a gaseous methylamine stream. After evaporation to dryness, the residue is taken up into ether and filtered, to give 5.6 g (86%) of product, M.p. 233°-235° C.
후처리
- customAfter evaporation to dryness
- filtrationfiltered
출처 및 근거
- ORD 기록
- ord-b61f206962e54c0791738650f81f1812
- 출처 데이터셋
- uspto-grants-1980_06
- 특허 번호
- US04208420
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