Nitroethane → HCID 3263891, 화합물

HRID 1706849

반응식

HRID 1706849 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][C:11]([CH:13]=O)=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.N1CCCCC1.[N+:21]([CH2:24][CH3:25])([O-:23])=[O:22]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][C:11]([CH:13]=[C:24]([N+:21]([O-:23])=[O:22])[CH3:25])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1

참가 물질

4

반응물 3

HCID 6587NitroethaneHCID 8082PiperidineHCID 6761845-(4-Chlorophenyl)-2-furaldehyde

생성물 1

HCID 3263891HCID 3263891, 화합물

실험 절차

A mixture of 82 g (0.4 mole) of 5-(p-chlorophenyl)-2-furaldehyde in 400 ml of nitroethane together with 4 ml of piperidine was heated at reflux for 2 hours.

후처리

  1. temperaturewas heated
  2. temperatureat reflux for 2 hours

출처 및 근거

ORD 기록
ord-6d59dc8dceaa4ae5a1db66d4b6e43768
출처 데이터셋
uspto-grants-1980_06
특허 번호
US04209448

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