Water → 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-ol
반응식
[CH2:1]1[O:9][C:8]2[CH:7]=[CH:6][C:5]([CH:10]=[CH:11][C:12](=[O:20])[CH2:13][N:14]3[CH2:19][CH2:18][O:17][CH2:16][CH2:15]3)=[CH:4][C:3]=2[O:2]1.O>CO>[CH2:1]1[O:9][C:8]2[CH:7]=[CH:6][C:5]([CH:10]=[CH:11][CH:12]([OH:20])[CH2:13][N:14]3[CH2:15][CH2:16][O:17][CH2:18][CH2:19]3)=[CH:4][C:3]=2[O:2]1참가 물질
4
실험 절차
27.5 g of the ketone (0.1 M) obtained in Example 1 is dissolved in 300 cm3 of methanol and an aqueous solution of KBH4 is added dropwise. The reaction mixture is left overnight and decomposed with water. The product obtained is filtered and recrystallised in ethanol.
후처리
- additionan aqueous solution of KBH4 is added dropwise
- customThe product obtained
- filtrationis filtered
- customrecrystallised in ethanol
출처 및 근거
- ORD 기록
- ord-842c2a0ae5a34c11a258e3a737fab6a7
- 출처 데이터셋
- uspto-grants-1980_06
- 특허 번호
- US04209517
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