반응식
[CH2:1]([O:3][C:4](=[O:16])[CH2:5][N:6]1[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=2[NH:8][C:7]1=[O:15])[CH3:2].Cl[CH2:18][C:19]1[CH:28]=[CH:27][C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[CH:20]=1>>[CH2:1]([O:3][C:4](=[O:16])[CH2:5][N:6]1[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=2[N:8]([CH2:18][C:19]2[CH:28]=[CH:27][C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH:20]=2)[C:7]1=[O:15])[CH3:2]참가 물질
3
실험 절차
The procedure described in Example 1 was repeated (using the same molar proportions as before) except that 440 mg. (0.002 mole) of 2-oxo-1-benzimidazolineacetic acid ethyl ester and 353 mg. (0.002 mole) of 2-chloromethylnaphthalene were reacted to afford 583 mg. (81%) of 3-(β-naphthyl)methyl-2-oxo-1-benzimidazolineacetic acid ethyl ester, isolated as an oil.
후처리
- customto afford 583 mg
출처 및 근거
- ORD 기록
- ord-a280e0fc7436444d8d1a83b9220f6b67
- 출처 데이터셋
- uspto-grants-1980_06
- 특허 번호
- US04209527
연결된 노트
불러오는 중…