2-(3-(Prop-1-en-2-yl)phenyl)propan-2-amine → 1-Methyl-1-[3-(1-methylethyl)phenyl]ethylamine
반응식
[CH3:1][C:2]([NH2:13])([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([C:10]([CH3:12])=[CH2:11])[CH:5]=1)[CH3:3]>C(O)C.[Pt]=O>[CH3:3][C:2]([NH2:13])([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:11])[CH3:12])[CH:5]=1)[CH3:1]참가 물질
4
실험 절차
First, 0.5 g of platinum oxide was added to a solution formed by dissolving 25.3 g of 1-methyl-1-[3-(1-methylethenyl)phenyl]ethylamine in 100 ml of ethyl alcohol, and a hydrogenation reaction was then carried out at a temperature of 15° to 35° C. for 7 hours under atmospheric pressure under a hydrogen gas stream. Afterward, reaction residues were removed by filtration, and the resultant filtrate was then concentrated to obtain 25.0 g of 1-methyl-1-[3-(1-methylethyl)phenyl]ethylamine.
후처리
- customformed
- customa hydrogenation reaction
- customAfterward, reaction residues
- customwere removed by filtration
- concentrationthe resultant filtrate was then concentrated
출처 및 근거
- ORD 기록
- ord-7a6cb0e023ff424598a8b15998185638
- 출처 데이터셋
- uspto-grants-1994_10
- 특허 번호
- US05352655
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