Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperazine → 1-[2-(4-Pyridinyl)ethyl]piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperazine | HCID 4837 | — |
| 반응물 | 4-Vinylpyridine | HCID 7502 | — |
| 생성물 | 1-[2-(4-Pyridinyl)ethyl]piperazine | HCID 558685 | 40.1% |
반응 단계
To a melt of piperazine (15 g, 0.17 mol) heated to 105° C. was added dropwise 4-vinylpyridine (1.25 mL, 0.012 mol). After refluxing the reaction for 5.5 hours, it was cooled to room temperature and chromatographed to provide 0.92 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05354747 |
| 출처 데이터셋 | uspto-grants-1994_10 |
| ORD ID | ord-d993ab5620a446f4b33f5a57a94925a0 |
| 출처 메모 | uspto-grants-1994_10 |