홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Triethylamine → HCID 131718743, 화합물

HRID 1708262
노트
인쇄 미리보기

반응식

HRID 1708262 반응식
C([N:3]([CH2:6][CH3:7])CC)C.[C:8]([NH:15][C@H:16]([C:21]([OH:23])=O)[CH2:17][CH2:18][S:19][CH3:20])([O:10][C:11]([CH3:14])([CH3:13])[CH3:12])=[O:9].ClC(OCC)=O.CC1[CH2:36][CH:35](N)[CH:34]([CH:38]([CH3:40])[CH3:39])[CH2:33][CH2:32]1>C1COCC1>[C:6]1([NH:3][C:21](=[O:23])[C@H:16]([CH2:17][CH2:18][S:19][CH3:20])[NH:15][C:8]([O:10][C:11]([CH3:12])([CH3:13])[CH3:14])=[O:9])([CH3:7])[CH2:36][CH2:35][CH:34]([CH:38]([CH3:40])[CH3:39])[CH2:33][CH2:32]1
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 8471TriethylamineHCID 10928Ethyl chloroformateHCID 894972-(Isopropyl)-5-methylcyclohexylamineHCID 89857Boc-L-methionine

생성물 1

HCID 131718743HCID 131718743, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

반응 조건

온도
-12 °C

실험 절차

0.45 mol of triethylamine is added to 0.45 mol of N-BOC-L-methionine in 1 l of THF at 0° C. The mixture is cooled to -12° C., and 0.45 mol of ethyl chloroformate is added dropwise. Stirring at -12° C. is continued for 20 minutes, and 0.45 mol of L-menthylamine is added dropwise. Stirring at 0° C. is continued for 45 minutes, and the mixture is then allowed to warm to room temperature.

후처리

  1. stirringStirring at 0° C.
  2. waitis continued for 45 minutes
  3. temperatureto warm to room temperature

출처 및 근거

ORD 기록
ord-af17f779df50479f95cd5bae5b6cc5bc
출처 데이터셋
uspto-grants-1994_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05357001

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트