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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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5alpha-Androst-7-ene-3-one-17beta-ol → 5alpha-Androst-8(14)-ene-3-one-17beta-ol

HRID 1708904
노트
인쇄 미리보기

반응식

HRID 1708904 반응식
[CH3:1][C@:2]12[CH2:19][CH2:18][C@H:17]3[C:7](=[CH:8][CH2:9][C@@H:10]4[C@:15]3([CH3:16])[CH2:14][CH2:13][C:12](=[O:20])[CH2:11]4)[C@@H:6]1[CH2:5][CH2:4][C@@H:3]2[OH:21]>C(OCC)(=O)C.[Pd]>[CH3:1][C@:2]12[CH2:19][CH2:18][C@H:17]3[C:7]([CH2:8][CH2:9][C@@H:10]4[C@:15]3([CH3:16])[CH2:14][CH2:13][C:12](=[O:20])[CH2:11]4)=[C:6]1[CH2:5][CH2:4][C@@H:3]2[OH:21]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 1

HCID 186380785alpha-Androst-7-ene-3-one-17beta-ol

생성물 1

HCID 186380795alpha-Androst-8(14)-ene-3-one-17beta-ol

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 8857Ethyl Acetate용매

실험 절차

A solution of 5α-androst-7-ene-3-one-17β-ol in ethyl acetate is hydrogenated at room temperature and 1 atmosphere over 10% palladium on carbon for 8 hours. Filtration to remove the catalyst and concentration affords 5α-androst-8(14)-ene-3-one-17β-ol.

후처리

  1. customis hydrogenated at room temperature
  2. filtrationFiltration
  3. customto remove
  4. concentrationthe catalyst and concentration

출처 및 근거

ORD 기록
ord-3c63eb8d022f475092314b70b3ab5711
출처 데이터셋
uspto-grants-1990_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04946834

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