Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,2,3,3,3-Pentafluoropropanol → 2,2,3,3,3-Pentafluoropropyl p-Toluenesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,2,3,3,3-Pentafluoropropanol | HCID 9872 | — |
| 반응물 | 3,3-Dichloro-1,1,1,2,2-pentafluoropropane | HCID 61112 | — |
| 반응물 | HCID 22024621 | HCID 22024621 | — |
| 생성물 | 2,2,3,3,3-Pentafluoropropyl p-Toluenesulfonate | HCID 2776017 | — |
반응 단계
These solvents are readily prepared from commercially available materials by standard and well-known organic syntheses techniques. For example, to prepare 1,1-dichloro-2,2,3,3,3-pentafluoropropane, 2,2,3,3,3-pentafluoro-1-propanol and p-toluenesulfonate chloride are reacted together to form 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate. Then, N-methylpyrrolidone, lithium chloride, and the 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate are reacted together to form 1-chloro-2,2,3,3,3-pentafluoropropane. Chlorine and the 1-chloro-2,2,3,3,3-pentafluoropropane are then reacted together to form 1,1-dichloro-2,2,3,3,3-pentafluoropropane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04947881 |
| 출처 데이터셋 | uspto-grants-1990_08 |
| ORD ID | ord-fd5e7776f6114c9bb172235745d63b99 |
| 출처 메모 | uspto-grants-1990_08 |