Chlorine → HCID 53813951, 화합물

HRID 1709089노트

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[Cl:1]Cl.[Cl:3][CH2:4][C:5]([F:14])([F:13])[C:6]([F:12])([F:11])[C:7]([F:10])([F:9])[F:8]>>[Cl:3][CH:4]([Cl:1])[C:5]([F:13])([F:14])[C:6]([F:11])([F:12])[C:7]([F:9])([F:8])[F:10]

참가 물질

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HCID 24526Chlorine

HCID 1362181,1,1,2,2,3,3-Heptafluoro-4-chlorobutane

생성물 1

HCID 53813951HCID 53813951, 화합물

실험 절차

For example, to prepare 1,1-dichloro-2,2,3,3,4,4,4-heptafluorobutane, 2,2,3,3,4,4,4-heptafluorobutanol and p-toluenesulfonyl chloride are reacted to form 2,2,3,3,4,4,4-heptafluorobutyl-p-toluenesulfonate. Then, N-methylpyrrolidone, lithium chloride, and the 2,2,3,3,4,4,4-heptafluorobutyl-p-toluenesulfonate are reacted to form 1-chloro-2,2,3,3,4,4,4-heptafluorobutane. Finally, chlorine and the 1-chloro-2,2,3,3,4,4,4-heptafluorobutane are reacted to form the 1,1-dichloro-2,2,3,3,4,4,4-heptafluorobutane.

출처 및 근거

ORD 기록: ord-5df46f70bea549edac96dfb155c176f8
출처 데이터셋: uspto-grants-1990_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04947881

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