2-(Thiophen-3-yl)acetaldehyde → (3-Thiophen-3-yl-phenyl)-acetaldehyde

HRID 1713671노트

반응식

HRID 1713671 반응식
S1C=CC(CC=O)=C1.[S:9]1[CH:13]=[CH:12][C:11]([C:14]2[CH:15]=[C:16]([CH2:20][CH2:21][OH:22])[CH:17]=[CH:18][CH:19]=2)=[CH:10]1>C(Cl)Cl.CCOCC>[S:9]1[CH:13]=[CH:12][C:11]([C:14]2[CH:15]=[C:16]([CH2:20][CH:21]=[O:22])[CH:17]=[CH:18][CH:19]=2)=[CH:10]1

참가 물질

4

반응물 2

HCID 141408302-(Thiophen-3-yl)acetaldehydeHCID 199171332-(3-Thiophen-3-yl-phenyl)-ethanol

생성물 1

HCID 58923511(3-Thiophen-3-yl-phenyl)-acetaldehyde

시약·촉매·용매 1

HCID 21881112Ethyl ether methylene chloride용매

실험 절차

The title compound is prepared as described in Example 12 (Procedure B) for 3-thiophenylacetaldehyde but using 2-(3-thiophen-3-yl-phenyl)-ethanol. The title compound: ES-MS: 200.9 [M−H]−; single peak at tR=4.53 min (System 2); Rf=0.63 (CH2Cl2/Et2O, 95/5).

후처리

  1. customThe title compound is prepared

출처 및 근거

ORD 기록
ord-ba154b68de2c44cb8bb2ffc9ab34776c
출처 데이터셋
uspto-grants-2010_09
특허 번호
US07795288B2

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