Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Octanol → Dicaprylyl Ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Octanol | HCID 957 | — |
| 반응물 | Sulfosuccinic acid monosodium salt | HCID 21220 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Dicaprylyl Ether | HCID 12399 | — |
반응 단계
206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05503760 |
| 출처 데이터셋 | uspto-grants-1996_04 |
| ORD ID | ord-e296b566e6b848bf9c01de3be92734cb |
| 출처 메모 | uspto-grants-1996_04 |