1-Octanol → Dicaprylyl Ether

HRID 1719986

반응식

HRID 1719986 반응식
[CH2:1]([OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S([CH:14]([CH2:18][C:19](O)=O)[C:15](O)=O)(O)(=O)=O>O>[CH2:1]([O:9][CH2:15][CH2:14][CH2:18][CH2:19][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 9571-OctanolHCID 21220Sulfosuccinic acid monosodium salt

생성물 1

HCID 12399Dicaprylyl Ether

시약·촉매·용매 1

HCID 962Water용매

실험 절차

206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.

후처리

  1. customformed
  2. distillationwas distilled off
  3. addition10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization
  4. washafter which the crude product was washed until neutral and
  5. distillationthen distilled

출처 및 근거

ORD 기록
ord-e296b566e6b848bf9c01de3be92734cb
출처 데이터셋
uspto-grants-1996_04
특허 번호
US05503760

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