Sodium Sulfite → HCID 86749374, 화합물
반응식
[F:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6]Br)=[C:4]([N+:10]([O-:12])=[O:11])[CH:3]=1.[S:13]([O-:16])([O-:15])=[O:14].[Na+:17].[Na+]>O>[F:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][S:13]([O-:16])(=[O:15])=[O:14])=[C:4]([N+:10]([O-:12])=[O:11])[CH:3]=1.[Na+:17]참가 물질
4
실험 절차
A solution of 4-fluoro-2-nitrobenzylbromide (50.1 g) and sodium sulfite (27.3 g) in water (200 ml) was heated under reflux for 2.5 hours and cooled to room temperature. The solvent was removed under reduced pressure and ethanol (100 ml) was added to the crude product.
후처리
- temperatureunder reflux for 2.5 hours
- customThe solvent was removed under reduced pressure and ethanol (100 ml)
- additionwas added to the crude product
출처 및 근거
- ORD 기록
- ord-d2b5e084fb4946508147eb1d65cfcb51
- 출처 데이터셋
- uspto-grants-1996_04
- 특허 번호
- US05504095
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