Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dioxane, 2-(2-bromoethyl)- → N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| 반응물 | 4-(4-Methylstyryl)quinoline | HCID 54172084 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide | HCID 70262692 | 70% |
반응 단계
4-(4-methylstyryl) quinoline (0.245 g) and 2-(2-bromoethyl) 1,3-dioxane (0.195 g) were mixed and refluxed in ethylacetate (1.5 ml) for 18 hours. Yellow-green precipitate was separated by filtration, washed with ethyl ether and dried in vacuo to give 0.308 g of N-[2-(1,3-dioxane-2-yl) ethyl]-4-(4-methylstyryl)-quinolinium bromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05506089 |
| 출처 데이터셋 | uspto-grants-1996_04 |
| ORD ID | ord-a0d0dfdda27248d287e139f8c23622fa |
| 출처 메모 | uspto-grants-1996_04 |