Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3,4-Dichlorophenoxy)acetic acid → HCID 18603269, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| 반응물 | Cyclohexanamine, N-methyl-2-(1-pyrrolidinyl)-, trans- | HCID 13377463 | — |
| 생성물 | HCID 18603269 | HCID 18603269 | — |
반응 단계
The title compound was prepared according to the method described in Example 2, using 3,4-dichlorophenoxyacetic acid (2.34 g, 11 mmol) and (±)-trans-N-methyl-N-[2-(1-pyrrolidinyl)cyclohexyl]amine prepared in Example 1 (2 g, 11 mmol). The crude product, which started to precipitate before the addition of the diethyl ether, was recrystallised from hot dichloromethane. Yield 2.9 g (62%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05506257 |
| 출처 데이터셋 | uspto-grants-1996_04 |
| ORD ID | ord-f450219564a54cf28b79e61e172337c4 |
| 출처 메모 | uspto-grants-1996_04 |