4-(Phenylmethyl)phenyl diethylcarbamate → 2-(1-Oxo-5-phenoxypentyl)-4-(phenylmethyl)phenyl diethylcarbamate

HRID 1721382노트

반응식

HRID 1721382 반응식
[CH2:1]([N:3]([CH2:20][CH3:21])[C:4](=[O:19])[O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:8][CH:7]=1)[CH3:2].CON(C)[C:25](=[O:37])[CH2:26][CH2:27][CH2:28][CH2:29][O:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1>>[CH2:20]([N:3]([CH2:1][CH3:2])[C:4](=[O:19])[O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:8][C:7]=1[C:25](=[O:37])[CH2:26][CH2:27][CH2:28][CH2:29][O:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1)[CH3:21]

참가 물질

3

반응물 2

HCID 224149984-(Phenylmethyl)phenyl diethylcarbamateHCID 22415008N-methoxy-N-methyl-5-phenoxypentanamide

생성물 1

HCID 538545992-(1-Oxo-5-phenoxypentyl)-4-(phenylmethyl)phenyl diethylcarbamate

실험 절차

The title compound was prepared from 4-(phenylmethyl)phenyl diethylcarbamate and N-methoxy-N-methyl-5-phenoxypentanamide following the same procedure used in Example F. NMR (CDCl3) δ1.18 (t, 3H), 1.26 (t, 3H), 1.83 (m, 4H), 2.92 (t, 2H), 3.35 (q, 2H), 3.45 (q, 2H) 3.99 (m, 4H), 6.86-7.31 (m, 12H), 7.49 (d, 1H).

출처 및 근거

ORD 기록
ord-f1ecce7a2c694ef58dad4d9d5baeb7ca
출처 데이터셋
uspto-grants-1996_04
특허 번호
US05510375

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