Ethanol → Ethyl sulfoacetate

HRID 1721388

반응식

HRID 1721388 반응식
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

참가 물질

3

반응물 2

HCID 702EthanolHCID 31257Sulfoacetic acid

생성물 1

HCID 12216623Ethyl sulfoacetate

실험 절차

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

후처리

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

출처 및 근거

ORD 기록
ord-25099fe8278a4bf3ab4105d4b60c77d8
출처 데이터셋
uspto-grants-1996_04
특허 번호
US05510379

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